8) respectively after 10 washes
Similar Hammett parameters across the different fluorinating reagents revealed the mechanisms of fluorination to be similar in each case. The 1 steroids,3 diaryl 1 steroids,3 dicarbonyl compounds delivered a convenient, sensitive spectrophotometric reporter of reactivity that also led to the discovery of a unique form of tautomeric polymorphism. Given the pharmaceutical relevance of, difluoroketonic compounds steroids, kinetics studies were performed on keto enol tautomerism and difluorination of 1,3 dicarbonyl systems to understand the factors that determine selectivity between mono and di fluorination.
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